(η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron

Base Information

Chemical Name:(η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron
CAS No.:108473-77-4
Molecular Formula:C₁₀H₁₁ClFeO₃Si
Molecular Weight:298.581
Hs Code.:

Synonyms:(η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron

Suppliers and Price of (η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron

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Technology Process of (η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron

There total 1 articles about (η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 87965-49-9
(1,1,3,4-tetramethyl-1-sila-2,4-cyclopentadiene)tricarbonyliron

: 7646-78-8
tin(IV) chloride

: 108473-77-4
(η4-exo-1-chloro-endo-1-methyl-3,4-dimethylsilole)tricarbonyliron

: 993-16-8
methyltin(IV) trichloride

Guidance literature:: In toluene; (N2); SnCl4 added to soln. of Fe complex at 0 °C; soln. stirred for 12 h at room temp.; solvent pumped off; residue taken up in hexane; filtration; several crysts. at -20 °C; elem. anal.; from the mother liquors, after evapn., CH3SnCl3 obtained by sublimation and identified by its 1H NMR spectrum and its m.p.;
DOI:10.1021/om00150a005