Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester

Base Information

Chemical Name:Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester
CAS No.:109912-60-9
Molecular Formula:C₂₃H₂₃NO₅S
Molecular Weight:425.505
Hs Code.:

Synonyms:Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester

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Chemical Property of Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester

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Technology Process of Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester

There total 1 articles about Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.6%

: 124-63-0
methanesulfonyl chloride

: 75986-02-6
α-amino-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester HCl

: 109912-60-9
Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester

Guidance literature:: With sodium hydrogencarbonate; triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/0223-5234(87)90014-6

Reference yield: 61.0%

: 109912-60-9
Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester

: 75-31-0
isopropylamine

: 109912-61-0
N-(1-methylethyl)-α-(methylsulfonyl)amino-4-(phenylmethoxy)benzeneacetamide

Guidance literature:: for 96h; Ambient temperature;
DOI:10.1016/0223-5234(87)90014-6

Reference yield:

: 109912-60-9
Sa-<(methylsulfonyl)amino>-4-(phenylmethoxy)benzeneacetic acid phenylmethyl ester

: 109912-57-4
N-<1-(4-hydroxyphenyl)>-2-<(1-methylethyl)amino>ethylmethanesulfonamide acetic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / 96 h / Ambient temperature

2: 44.8 percent / 1.) BH₃*Me₂S; 2.) HCl / 1.) THF, 0 deg C, 1 h, r. t., 30 min, reflux 6 h; 2.) EtOAc

3: 1.) H₂ / 1.) 10percent Pd/C / 1.) MeOH, 50 psi, 4 h; 2.) H₂O, Bio-Rex 70 resin

With hydrogenchloride; dimethylsulfide borane complex; hydrogen; palladium on activated charcoal;
DOI:10.1016/0223-5234(87)90014-6