4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

Base Information

Chemical Name:4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane
CAS No.:177089-50-8
Molecular Formula:C₃₀H₄₈N₄O₈S₂
Molecular Weight:656.865
Hs Code.:

Synonyms:4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

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Chemical Property of 4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

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Technology Process of 4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

There total 6 articles about 4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 115942-18-2
4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

: 177089-50-8
4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; Ambient temperature;
DOI:10.1021/jo952283x

Reference yield:

: 132930-16-6
1,11-diphthalimido-6-(4-tolylsulphonyl)-3,9-dioxa-6-azaundecane

: 177089-50-8
4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / hydrazine hydrate / ethanol / 5 h / Heating

2: benzene / 4 h / Heating

3: H₂ / PtO₂ / acetic acid / 6 h / Ambient temperature

4: 45 percent / Na₂CO₃ / acetonitrile / 96 h / Heating

5: 87 percent / H₂ / Pd/C / acetic acid / Ambient temperature

With hydrogen; sodium carbonate; hydrazine hydrate; platinum(IV) oxide; palladium on activated charcoal; In ethanol; acetic acid; acetonitrile; benzene;
DOI:10.1021/jo952283x

Reference yield:

: 132930-17-7
6-(4-tolylsulphonyl)-3,9-dioxa-6-azaundecane-1,11-diamine

: 177089-50-8
4,16-di[(4-methylphenyl)sulfonyl]-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / 4 h / Heating

2: H₂ / PtO₂ / acetic acid / 6 h / Ambient temperature

3: 45 percent / Na₂CO₃ / acetonitrile / 96 h / Heating

4: 87 percent / H₂ / Pd/C / acetic acid / Ambient temperature

With hydrogen; sodium carbonate; platinum(IV) oxide; palladium on activated charcoal; In acetic acid; acetonitrile; benzene;
DOI:10.1021/jo952283x