4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

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Chemical Name:4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane
CAS No.:115942-18-2
Molecular Formula:C₄₄H₆₀N₄O₈S₂
Molecular Weight:837.114
Hs Code.:

Synonyms:4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

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Chemical Property of 4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

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Technology Process of 4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

There total 8 articles about 4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 80639-61-8
6-<(4-methylphenyl)sulfonyl>-3,9-dioxa-6-aza-1,11-undecanediol bis(methanesulfonate)

: 177089-48-4
N,N-Bis-[2-(2-benzylamino-ethoxy)-ethyl]-4-methyl-benzenesulfonamide

: 115942-18-2
4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

Guidance literature:: With sodium carbonate; In acetonitrile; for 96h; Heating;
DOI:10.1021/jo952283x

Reference yield: 4.7%

: 80639-61-8
6-<(4-methylphenyl)sulfonyl>-3,9-dioxa-6-aza-1,11-undecanediol bis(methanesulfonate)

: 100-46-9
benzylamine

: 80639-62-9
10-benzyl-4-<(4-methylphenyl)sulfonyl>-1,7-dioxa-4,10-diazacyclododecane

: 115942-18-2
4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

Guidance literature:: With sodium carbonate; In acetonitrile; for 40h; Heating;
DOI:10.1021/jo00257a016

Reference yield:

: 132930-17-7
6-(4-tolylsulphonyl)-3,9-dioxa-6-azaundecane-1,11-diamine

: 115942-18-2
4,16-di-p-toluenesulfonyl-10,22-dibenzyl-1,7,13,19-tetraoxa-4,10,16,22-tetraazacyclotetracosane

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 4 h / Heating

2: H₂ / PtO₂ / acetic acid / 6 h / Ambient temperature

3: 45 percent / Na₂CO₃ / acetonitrile / 96 h / Heating

With hydrogen; sodium carbonate; platinum(IV) oxide; In acetic acid; acetonitrile; benzene;
DOI:10.1021/jo952283x