Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester
CAS No.:178751-61-6
Molecular Formula:C₂₁H₃₆O₄SSi₂
Molecular Weight:440.751
Hs Code.:

Synonyms:Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester

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Technology Process of Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester

There total 3 articles about Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 178751-54-7
(S)-2-hydroxy-5-trimethylsilyl-1-p-toluenesulfonyloxy-4-pentyne

: 178751-61-6
Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 16h; Ambient temperature;

Reference yield:

: 70987-78-9,6746-81-2
(S)-Glycidyl tosylate

: 178751-61-6
Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, 2.) BF₃*OEt₂

2: 91 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

With 1H-imidazole; n-butyllithium; boron trifluoride diethyl etherate; In N,N-dimethyl-formamide;

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 178751-61-6
Toluene-4-sulfonic acid (S)-2-(tert-butyl-dimethyl-silanyloxy)-5-trimethylsilanyl-pent-4-ynyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, 2.) BF₃*OEt₂

2: 91 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

With 1H-imidazole; n-butyllithium; boron trifluoride diethyl etherate; In N,N-dimethyl-formamide;