4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid

Base Information

Chemical Name:4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid
CAS No.:128745-68-6
Molecular Formula:C₂₃H₂₂O₈
Molecular Weight:426.423
Hs Code.:

Synonyms:4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid

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Chemical Property of 4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid

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Technology Process of 4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid

There total 1 articles about 4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 109930-06-5
4-(3,5-di-O-benzoyl-1,4-anhydro-2-deoxy-D-erythro-pent-1-enofuranosyl)-4-oxo-2-butenoic acid

: 128745-68-6
4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid

: 128745-69-7
4-(3,5-di-O-benzoyl-2-deoxy-α-D-erythro-pentofuranosyl)-4-oxobutyric acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 12h; under 760 Torr;

Reference yield: 96.0%

: 67-56-1
methanol

: 128745-68-6
4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid

: 128745-70-0
methyl 4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyrate

Guidance literature:: With hydrogenchloride; for 12h; Ambient temperature;

Reference yield:

: 128745-68-6
4-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4-oxobutyric acid

: 128745-72-2
3-(3,5-di-O-benzoyl-2-deoxy-β-D-erythro-pentofuranosyl)-4,5-dihydropyridazin-6(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / HCl / 12 h / Ambient temperature

2: 74 percent / hydrazine monohydrate / methanol / 12 h / Ambient temperature

With hydrogenchloride; hydrazine hydrate; In methanol;