N⁴-cyclohexyl-N⁵-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine

Base Information

• Chemical Name: N⁴-cyclohexyl-N⁵-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine
• CAS No.: 613222-37-0
• Molecular Formula: C₂₇H₃₁N₅O₂
• Molecular Weight: 457.575

Synonyms:N⁴-cyclohexyl-N⁵-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine

Chemical Property of N⁴-cyclohexyl-N⁵-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine

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Technology Process of N⁴-cyclohexyl-N⁵-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine

There total 1 articles about N⁴-cyclohexyl-N⁵-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

Cyclohexyl isocyanide (931-53-3) + N-(p-nitrophenyl)benzohydrazonoyl chloride (25939-13-3) → 1,4-bis-(4-nitrophenyl)-3,6-diphenyl-1,4-dihydro-1,2,4,5-tetrazine (69374-53-4) + N4-cyclohexyl-N5-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine (613222-37-0) + cyclohexyl-{2-(4-nitro-phenyl)-4-[1-(4-nitro-phenyl)-3-phenyl-1,2,4-triaza-spiro[4.5]dec-2-en-4-yl]-5-phenyl-2H-pyrazol-3-yl}-amine (613222-26-7) + 4-cyclohexyl-1-(4-nitrophenyl)-5-[(4-nitrophenyl{[(4-nitrophenyl)hydrazono](phenyl)methyl}hydrazono)(phenyl)methyl]-3-phenyl-1H-1,2,4-triazol-4-ium chloride

Guidance literature:

With triethylamine; In benzene; for 1h; Further byproducts given; Heating;

DOI:10.1002/jhet.5570400411

Reference yield: 74.0%

N4-cyclohexyl-N5-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine (613222-37-0) → N4-cyclohexyl-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine

Guidance literature:

With ethanol; at 20 ℃; for 24h;

DOI:10.1002/jhet.5570400411

Reference yield: 40.0%

N-(p-nitrophenyl)benzohydrazonoyl chloride (25939-13-3) + N4-cyclohexyl-N5-cyclohexylidene-1-(4-nitrophenyl)-3-phenylpyrazole-4,5-diamine (613222-37-0) → N-cyclohexyl-1-(4-nitrophenyl)-5-[1-(nitrophenyl)-3-phenyl-1,2,4-triazaspiro[4.5]dec-2-en-4-yl]-3-phenylpyrazol-4-amine

Guidance literature:

With triethylamine; In benzene; for 0.166667h; Heating;

DOI:10.1002/jhet.5570400411

upstream raw materials:

Cyclohexyl isocyanide

N-(p-nitrophenyl)benzohydrazonoyl chloride

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