N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide

Base Information

Chemical Name:N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide
CAS No.:1415729-98-4
Molecular Formula:C₂₀H₂₂AsN₅O₄S₂
Molecular Weight:535.479
Hs Code.:

Synonyms:N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide

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Chemical Property of N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide

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Technology Process of N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide

There total 8 articles about N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5577-20-8
4-(1,3,2-dithiocycloarsenic-2-yl)aniline

: 88235-25-0
6-(7-nitrobenzofurazan-4-ylamino)hexanoic acid

: 1415729-98-4
N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201300567

Reference yield: 33.0%

: 1334715-64-8
N-(4-(1,3,2-dithiarsolan-2-yl)phenyl)-6-aminohexanamide

: 10199-89-0
NBD chloride

: 1415729-98-4
N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide

Guidance literature:: With potassium carbonate; triethylamine; In dichloromethane; acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201300567

Reference yield:

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 1415729-98-4
N-[4-(1,3,2-dithiarsolan-2-yl)phenyl]-6-[(7-nitrobenzo[c][1,2,5]oxadiazol-4-yl)amino]hexanamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / tetrahydrofuran; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

3: triethylamine; potassium carbonate / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

With potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201300567