1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide

Base Information

Chemical Name:1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide
CAS No.:1380921-10-7
Molecular Formula:C₁₃H₁₉ClN₄O
Molecular Weight:282.773
Hs Code.:

Synonyms:1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide

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Chemical Property of 1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide

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Technology Process of 1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide

There total 3 articles about 1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1380921-09-4
4-chloro-5-(2-dimethylcarbamoyl-pyrrolidin-1-yl)-2-nitroaniline

: 1380921-10-7
1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide

Guidance literature:: With tin(II) chloride dihdyrate; In ethyl acetate; for 3h; Reflux;

Reference yield:

: 6641-64-1
4,5-dichloro-2-nitroaniline

: 1380921-10-7
1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 2.5 h / 120 °C

2: tin(II) chloride dihdyrate / ethyl acetate / 3 h / Reflux

With tin(II) chloride dihdyrate; potassium carbonate; In dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 433980-61-1
proline-N,N-dimethylamide

: 1380921-10-7
1-(4,5-diamino-2-chloro-phenyl)-pyrrolidine-2-carboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 2.5 h / 120 °C

2: tin(II) chloride dihdyrate / ethyl acetate / 3 h / Reflux

With tin(II) chloride dihdyrate; potassium carbonate; In dimethyl sulfoxide; ethyl acetate;