N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Chemical Name:N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside
CAS No.:1319717-47-9
Molecular Formula:C₈₃H₉₆N₁₀O₁₈Si
Molecular Weight:1549.82
Hs Code.:

N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

Synonyms:N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Chemical Property of N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Technology Process of N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

There total 1 articles about N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1319717-45-7
N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

: 1319717-46-8
methyl (phenyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-1-thio-β-D-mannopyranosyl uronate)

: 1319717-47-9
N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

Guidance literature:: methyl (phenyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-1-thio-β-D-mannopyranosyl uronate); With 1,1'-sulfinylbisbenzene; In dichloromethane; toluene; at 20 ℃; for 0.333333h; Molecular sieve; Inert atmosphere; Large scale reaction;

With trifluoromethylsulfonic anhydride; In dichloromethane; toluene; at -80 - -60 ℃;

N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside; In dichloromethane; toluene; at -80 - -10 ℃; for 4h; stereoselective reaction;
DOI:10.1021/jo201179p