diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

Base Information

Chemical Name:diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate
CAS No.:1403478-02-3
Molecular Formula:C₁₆H₂₁N₃O₅
Molecular Weight:335.36
Hs Code.:

Synonyms:diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

Suppliers and Price of diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

Chemical Property:

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Technology Process of diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

There total 3 articles about diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 68843-67-4
1-phenyl-but-3-en-1-one oxime

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 1403478-02-3
diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

Guidance literature:: In toluene; at 50 ℃; for 20h; Inert atmosphere;
DOI:10.1002/anie.201203799

Reference yield:

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 1403478-02-3
diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 °C

3: toluene / 20 h / 50 °C / Inert atmosphere

With Jones reagent; hydroxylamine hydrochloride; sodium acetate; In diethyl ether; ethanol; water; toluene;
DOI:10.1002/anie.201203799

Reference yield:

: 100-52-7
benzaldehyde

: 1403478-02-3
diethyl 1-((3-phenyl-4,5-dihydroisoxazol-5-yl)methyl)hydrazine-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: indium / tetrahydrofuran; water / 20 °C

2: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

3: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 °C

4: toluene / 20 h / 50 °C / Inert atmosphere

With indium; Jones reagent; hydroxylamine hydrochloride; sodium acetate; In tetrahydrofuran; diethyl ether; ethanol; water; toluene;
DOI:10.1002/anie.201203799