1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

Base Information

Chemical Name:1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol
CAS No.:945393-05-5
Molecular Formula:C₃₄H₃₈O₄Si₂
Molecular Weight:566.844
Hs Code.:

Synonyms:1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

Suppliers and Price of 1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

There total 1 articles about 1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1066-54-2
trimethylsilylacetylene

: 801287-71-8
3,6-dimethoxy-3,6-diphenylocta-1,4,7-triyne-1,8-dial

: 945393-05-5
1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

Guidance literature:: trimethylsilylacetylene; With ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1h;

3,6-dimethoxy-3,6-diphenylocta-1,4,7-triyne-1,8-dial; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 3h; Further stages.;
DOI:10.1002/chem.200601191

Reference yield: 86.0%

: 945393-05-5
1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

: 6,9-dimethoxy-1,14-bis(trimethylsilyl)-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-dione

Guidance literature:: With manganese oxide; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/chem.200601191

Reference yield:

: 945393-05-5
1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol

: 333-27-7
methyl trifluoromethanesulfonate

: C₃₆H₄₂O₄Si₂

Guidance literature:: 1,14-bis(trimethylsily)-6,9-dimethoxy-6,9-diphenyltetradeca-1,4,7,10,13-pentayne-3,12-diol; With n-butyllithium; In diethyl ether; hexane; at -80 ℃; for 0.0166667h;

methyl trifluoromethanesulfonate; In diethyl ether; hexane; at -10 - 0 ℃; for 15h; Further stages.;
DOI:10.1002/chem.200601191