1-[(benzylamino)ethyl]-o-carborane hydrochloride

Base Information

• Chemical Name: 1-[(benzylamino)ethyl]-o-carborane hydrochloride
• CAS No.: 497858-99-8
• Molecular Formula: C₁₁H₂₃B₁₀N*ClH
• Molecular Weight: 313.881
• Mol file: 497858-99-8.mol

Synonyms:1-[(benzylamino)ethyl]-o-carborane hydrochloride

Chemical Property of 1-[(benzylamino)ethyl]-o-carborane hydrochloride

Chemical Property:

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Technology Process of 1-[(benzylamino)ethyl]-o-carborane hydrochloride

There total 1 articles about 1-[(benzylamino)ethyl]-o-carborane hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

hydrogenchloride (7647-01-0,15364-23-5) + 1-[(dibenzylamino)ethyl]-o-carborane (497858-94-3) → 1-[(benzylamino)ethyl]-o-carborane hydrochloride (497858-99-8)

Guidance literature:

With H₂; catalyst: Pd/C; In ethanol; under dry inert atm., Schlenk technique; mixt. of carborane, concd. HCl and catalyst under H2 atm. (60 psi) was shaken for 5 h at room temp.; ppt. was filtered, solvent was removed, residue was recrystd. from EtOH at -10°C; elem. anal.;

DOI:10.1021/om020803q

upstream raw materials:

hydrogenchloride

1-[(dibenzylamino)ethyl]-o-carborane