5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine

Base Information

Chemical Name:5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine
CAS No.:1417658-84-4
Molecular Formula:C₂₁H₁₇FN₂O₃
Molecular Weight:364.376
Hs Code.:

Synonyms:5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine

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Chemical Property of 5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine

Chemical Property:

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Technology Process of 5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine

There total 4 articles about 5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 367-12-4
2-fluorophenol

: 1417658-83-3
5-chloro-2-(4-methoxy-3,5-dimethyl phenyl)oxazolo[5,4-b]pyridine

: 1417658-84-4
5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 180 ℃; for 0.75h; Microwave irradiation;

Reference yield:

: 21668-34-8
3,5-dimethyl-4-methoxybenzoic acid chloride

: 1417658-84-4
5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 17 h / 0 - 20 °C

2: 1,10-Phenanthroline; copper(l) iodide; caesium carbonate / tetrahydrofuran / 2 h / 140 °C / Microwave irradiation

3: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 180 °C / Microwave irradiation

With pyridine; copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1417658-82-2
N-(2,6-dichloropyridin-3-yl)-4-methoxy-3,5-dimethylbenzamide

: 1417658-84-4
5-(2-fluorophenoxy)-2-(4-methoxy-3,5-dimethylphenyl)oxazolo[5,4-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 1,10-Phenanthroline; copper(l) iodide; caesium carbonate / tetrahydrofuran / 2 h / 140 °C / Microwave irradiation

2: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 180 °C / Microwave irradiation

With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;