(R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1570511-06-6
Molecular Formula:C₂₂H₂₉BO₃
Molecular Weight:352.281
Hs Code.:

Synonyms:(R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 7 articles about (R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 144479-03-8
1-phenyl-3-benzyloxy-1-propyne

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1570511-06-6
(R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With C₂₇H₃₀Br₂CoN₄; hydrogen; sodium triethylborohydride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 10h; Reagent/catalyst; Solvent; enantioselective reaction; Schlenk technique;
DOI:10.1021/jacs.7b09832

Reference yield: 74.0%

: 591-50-4
iodobenzene

: 1227056-28-1
2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 1570511-06-6
(R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (3aR,8aR)-N,N,2,2-tetramethyl-4,4,8,8-tetra-p-tolyltetrahydro-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-amine; palladium diacetate; potassium hydroxide; In 1,4-dioxane; at 20 ℃; for 12h; enantioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1021/ja500029w

Reference yield:

: 144479-03-8
1-phenyl-3-benzyloxy-1-propyne

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1570511-06-6
(R)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: (S)-2-(3-(benzyloxy)-1-phenylpropyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With C₂₆H₂₈Br₂CoN₄; hydrogen; sodium triethylborohydride; In diethyl ether; at 20 ℃; for 10h; Overall yield = 78 %Spectr.;
DOI:10.1021/jacs.7b09832