2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:1227056-28-1
Molecular Formula:C₂₂H₃₆B₂O₅
Molecular Weight:402.147
Hs Code.:

Synonyms:2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Chemical Property of 2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of 2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 2 articles about 2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1197-51-9
N-propargylbenzylamine

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1227056-28-1
2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; copper(l) chloride; sodium t-butanolate; In toluene; at 20 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

N-propargylbenzylamine; In toluene; at 20 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/asia.201402458

Reference yield: 70.0%

: 4981-83-3
2-(Benzyloxy)ethyl p-toluenesulfonate

: 73183-34-3
bis(pinacol)diborane

: 74-95-3
1,1-dibromomethane

: 1227056-28-1
2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With copper(l) iodide; lithium methanolate; triphenylphosphine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1021/ja500029w

Reference yield: 93.0%

: 1227056-28-1
2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 2,2'-(3-phenylpropane-1,1-diyl-1-d)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 143-15-7
1-dodecylbromide

: 4,4,5,5-tetramethyl-2-(1-phenylpentadecan-3-yl-3-d)-1,3,2-dioxaborolane

: 2-(1-(benzyloxy)pentadecan-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 2,2'-(3-(benzyloxy)propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane); 2,2'-(3-phenylpropane-1,1-diyl-1-d)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane); With sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 0.25h;

1-dodecylbromide; In tetrahydrofuran; at 20 ℃; for 3h; Sealed tube;
DOI:10.1021/ja505455z