Tris(4-ethoxyphenyl)bismuthane

Base Information

• Chemical Name: Tris(4-ethoxyphenyl)bismuthane
• CAS No.: 90591-48-3
• Molecular Formula: C24H27 Bi O3
• Molecular Weight: 572.457
• DSSTox Substance ID: DTXSID00533222
• Mol file: 90591-48-3.mol

Synonyms:90591-48-3;TRIS(4-ETHOXYPHENYL)BISMUTH;tris(4-ethoxyphenyl)bismuthane;TRIS(4-ETHOXYPHENYL)BISMUTHINE;tris(p-ethoxyphenyl)bismuthine;SCHEMBL5455733;DTXSID00533222;AMY18074;?TRIS(4-ETHOXYPHENYL)BISMUTH

Chemical Property of Tris(4-ethoxyphenyl)bismuthane

Chemical Property:

• Melting Point: 73 °C
• PSA: 27.69000
• LogP: 5.65650
• Storage Temp.: -20°C Freezer, Under inert atmosphere
• Solubility.: Chloroform (Slightly), Ethyl Acetate (Slightly)
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 9
• Exact Mass: 572.17642
• Heavy Atom Count: 28
• Complexity: 346

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tris(4-ethoxyphenyl)bismuthine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC1=CC=C(C=C1)[Bi](C2=CC=C(C=C2)OCC)C3=CC=C(C=C3)OCC
• Uses: Tris(4-ethoxyphenyl)bismuthine is used as a catalyst for olefin polymerization.

Technology Process of Tris(4-ethoxyphenyl)bismuthane

There total 5 articles about Tris(4-ethoxyphenyl)bismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.8%

bismuth(III) chloride (7787-60-2) + 4-ethoxyphenylmagnesium bromide (41842-30-2) → tris-(4-ethoxy-phenyl)-bismuthine (90591-48-3)

Guidance literature:

In diethyl ether;

DOI:10.1021/ja01874a047

Reference yield:

4-ethoxyphenylmagnesium bromide (41842-30-2) → tris-(4-ethoxy-phenyl)-bismuthine (90591-48-3)

Guidance literature:

With bismuth(III) chloride; diethyl ether;

DOI:10.1021/ja01874a047

Reference yield:

→ tris-(4-ethoxy-phenyl)-bismuthine (90591-48-3)

Guidance literature:

With bismuth;

upstream raw materials:

4-bromoethoxybenzene

4-ethoxyphenylmagnesium bromide

bismuth(III) chloride

Downstream raw materials:

(C₆H₄C₂H₅O)Bi(CF₃COO)2

(C₆H₄C₂H₅O)2Bi(CF₃COO)

2-(4-ethoxybenzyl)-3-(4-nitrophenyl) acrylic acid methyl ester

2-(4-ethoxybenzyl)-3-phenylacrylic acid methyl ester

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