1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Base Information

Chemical Name:1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane
CAS No.:149746-81-6
Molecular Formula:C₃₄H₄₆N₂O₁₂
Molecular Weight:674.745
Hs Code.:

Synonyms:1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

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Chemical Property of 1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

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Technology Process of 1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

There total 12 articles about 1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 105-36-2
ethyl bromoacetate

: 2-(5-Acetoxy-2-{2-[2-(bis-ethoxycarbonylmethyl-amino)-5-methyl-phenoxy]-ethoxy}-phenylamino)-propionic acid ethyl ester

: 149746-81-6
1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In acetonitrile; at 100 ℃;

Reference yield:

: 3233-32-7
hydroquinone monoacetate

: 149746-81-6
1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: Multi-step reaction with 5 steps

1: 43 percent / nitric acid, acetic acid / 0.17 h / 4 °C

2: 72 percent / aq. potassium carbonate / dimethylformamide / 1 h / 100 °C

3: H₂ / 10percent Pd/C / ethanol / 0.5 h

4: 1,8-bis(dimethylamino)naphthalene / acetonitrile / 6 h / 100 °C

5: 67 percent / 1,8-bis(dimethylamino)naphthalene / acetonitrile / 100 °C

With hydrogen; nitric acid; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium carbonate; acetic acid; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 58149-50-1
4-hydroxy-3-nitrophenyl acetate

: 149746-81-6
1-<4-acetoxy-2-<1-ethoxycarbonylethyl(ethoxycarbonylmethyl)amino>phenoxy>-2-<2-bis(ethoxycarbonylmethyl)amino-5-methylphenoxy>ethane

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / aq. potassium carbonate / dimethylformamide / 1 h / 100 °C

2: H₂ / 10percent Pd/C / ethanol / 0.5 h

3: 1,8-bis(dimethylamino)naphthalene / acetonitrile / 6 h / 100 °C

4: 67 percent / 1,8-bis(dimethylamino)naphthalene / acetonitrile / 100 °C

With hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium carbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; acetonitrile;