benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

Base Information

Chemical Name:benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate
CAS No.:1415124-85-4
Molecular Formula:C₁₇H₁₅N₃O₄
Molecular Weight:325.324
Hs Code.:

Synonyms:benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

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Chemical Property of benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

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Technology Process of benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

There total 10 articles about benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.13%

: 1415124-79-6
benzyl 4-amino-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

: 79-22-1
methyl chloroformate

: 1415124-85-4
benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; at -10 - 20 ℃; for 0.5h;

Reference yield: 49.13%

: 1426255-11-9
benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate

: 79-22-1
methyl chloroformate

: 1415124-85-4
benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; at -10 - 20 ℃; for 0.5h;

Reference yield:

: 108-99-6
3-Methylpyridine

: 1415124-85-4
benzyl 4-[(methoxycarbonyl)amino]-1H-pyrrolo[3,2-c]pyridine-1-carboxylate

Guidance literature:: Multi-step reaction with 9 steps

1.1: dihydrogen peroxide / acetic acid / 70 °C / Cooling with ice

2.1: nitric acid / sulfuric acid / 2 h / 0 - 100 °C

3.1: dimethyl amine / N,N-dimethyl-formamide / 15 h / 90 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 2 h

5.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; Dimethyl ether / 4 h / 20 °C

7.1: chloroform / 0.25 h

7.2: 1 h / 0 - 20 °C

8.1: trifluoroacetic acid / dichloromethane / 20 °C / Cooling with ice

9.1: triethylamine / tetrahydrofuran / 0.5 h / -10 - 20 °C

With hydrogen; dihydrogen peroxide; nitric acid; dimethyl amine; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; sulfuric acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; Dimethyl ether; dichloromethane; chloroform; acetic acid; N,N-dimethyl-formamide;