3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol

Base Information

• Chemical Name: 3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol
• CAS No.: 130883-72-6
• Molecular Formula: C₂₅H₂₂O₁₀
• Molecular Weight: 482.444
• Mol file: 130883-72-6.mol

Synonyms:3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol

Chemical Property of 3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol

There total 2 articles about 3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-methylsalicylic acid (83-40-9) + 3,3'-dicarboxy-4,4'-dihydroxy-5,5'-dimethyldiphenylmethane (2581-36-4) → 3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol (130883-72-6)

Guidance literature:

With sulfuric acid; sodium nitrite; for 16h; Ambient temperature;

DOI:10.1021/jm00105a053

Reference yield:

3-methylsalicylic acid (83-40-9) → 3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol (130883-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / 25percent H₂SO₄ / 12 h / 90 °C

2: 90 percent / concd. H₂SO₄, NaNO₂ / 16 h / Ambient temperature

With sulfuric acid; sodium nitrite;

DOI:10.1021/jm00105a053

Reference yield: 95.0%

3,3',3''-tricarboxy-4,4',4''-trihydroxy-5,5',5''-trimethyltriphenylcarbinol (130883-72-6) → 5,5',5''-tricarboxy-4,4',4''-trihydroxy-3,3',3''-trimethyltriphenylmethane (129749-43-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 48h; under 4550.9 Torr;

DOI:10.1021/jm00105a053

upstream raw materials:

3-methylsalicylic acid

3,3'-dicarboxy-4,4'-dihydroxy-5,5'-dimethyldiphenylmethane

Downstream raw materials:

4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylcarbinol

5,5',5''-tricarboxy-4,4',4''-trihydroxy-3,3',3''-trimethyltriphenylmethane

4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane