N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

Base Information

Chemical Name:N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam
CAS No.:278793-20-7
Molecular Formula:C₂₀H₂₆N₂O₅S
Molecular Weight:406.503
Hs Code.:

Synonyms:N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

Suppliers and Price of N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

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Chemical Property of N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

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Technology Process of N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

There total 7 articles about N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118992-89-5
[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]methanol

: 278793-20-7
N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

Guidance literature:: Multi-step reaction with 6 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: 9.0 g / Et₃N / CH₂Cl₂ / 8 h / Heating

3: hydrazine monohydrate / methanol / 1 h / 20 °C

4: 9.4 g / methanol / 8 h / 20 °C

5: 100 percent / Me₃Al / 1,2-dichloro-ethane; hexane / 24 h / Heating

6: 89 percent / pyridinium p-toluenesulfonate / ethanol / 2 h / 60 °C

With trimethylaluminum; pyridinium p-toluenesulfonate; hydrazine hydrate; triethylamine; In methanol; ethanol; hexane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.51.540

Reference yield:

: 278793-19-4
methyl (E)-2-[4-(t-butyldimethylsiloxymethyl)benzyloxyimino]ethanate

: 278793-20-7
N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Me₃Al / 1,2-dichloro-ethane; hexane / 24 h / Heating

2: 89 percent / pyridinium p-toluenesulfonate / ethanol / 2 h / 60 °C

With trimethylaluminum; pyridinium p-toluenesulfonate; In ethanol; hexane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.51.540

Reference yield:

: 278793-18-3
N-[4-(t-butyldimethylsiloxymethyl)benzyloxy]phthalimide

: 278793-20-7
N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine monohydrate / methanol / 1 h / 20 °C

2: 9.4 g / methanol / 8 h / 20 °C

3: 100 percent / Me₃Al / 1,2-dichloro-ethane; hexane / 24 h / Heating

4: 89 percent / pyridinium p-toluenesulfonate / ethanol / 2 h / 60 °C

With trimethylaluminum; pyridinium p-toluenesulfonate; hydrazine hydrate; In methanol; ethanol; hexane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.51.540