N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester

Base Information

Chemical Name:N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester
CAS No.:278793-22-9
Molecular Formula:C₂₅H₃₂N₂O₈S
Molecular Weight:520.604
Hs Code.:

Synonyms:N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester

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Chemical Property of N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester

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Technology Process of N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester

There total 9 articles about N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-55-4
glutaric anhydride,

: 278793-20-7
N-[(E)-2-[4-(hydroxymethyl)benzyloxyimino]ethanonyl]bornane-10,2-sultam

: 278793-22-9
N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester

Guidance literature:: With pyridine; at 80 ℃; for 4h;
DOI:10.1248/cpb.51.540

Reference yield:

: 118992-89-5
[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]methanol

: 278793-22-9
N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester

Guidance literature:: Multi-step reaction with 7 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: 9.0 g / Et₃N / CH₂Cl₂ / 8 h / Heating

3: hydrazine monohydrate / methanol / 1 h / 20 °C

4: 9.4 g / methanol / 8 h / 20 °C

5: 100 percent / Me₃Al / 1,2-dichloro-ethane; hexane / 24 h / Heating

6: 89 percent / pyridinium p-toluenesulfonate / ethanol / 2 h / 60 °C

7: 99 percent / pyridine / 4 h / 80 °C

With pyridine; trimethylaluminum; pyridinium p-toluenesulfonate; hydrazine hydrate; triethylamine; In methanol; ethanol; hexane; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.51.540

Reference yield:

: 278793-19-4
methyl (E)-2-[4-(t-butyldimethylsiloxymethyl)benzyloxyimino]ethanate

: 278793-22-9
N-[(E)-2-(4-(hydroxymethyl)benzyloxyimino)ethanonyl]bornane-10,2-sultam glutaric acid monoester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Me₃Al / 1,2-dichloro-ethane; hexane / 24 h / Heating

2: 89 percent / pyridinium p-toluenesulfonate / ethanol / 2 h / 60 °C

3: 99 percent / pyridine / 4 h / 80 °C

With pyridine; trimethylaluminum; pyridinium p-toluenesulfonate; In ethanol; hexane; 1,2-dichloro-ethane;
DOI:10.1248/cpb.51.540