C₂₃H₂₂FNO₄

Base Information

Chemical Name:C₂₃H₂₂FNO₄
CAS No.:1427406-54-9
Molecular Formula:C₂₃H₂₂FNO₄
Molecular Weight:395.43
Hs Code.:

C<sub>23</sub>H<sub>22</sub>FNO<sub>4</sub>

Synonyms:C₂₃H₂₂FNO₄

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Chemical Property of C₂₃H₂₂FNO₄

Chemical Property:

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Technology Process of C₂₃H₂₂FNO₄

There total 18 articles about C₂₃H₂₂FNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1427408-22-7
C₂₆H₂₈FNO₄

: 1427406-54-9
C₂₃H₂₂FNO₄

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 2198-53-0
N-(2,6-dimethylphenyl)acetamide

: 1427406-54-9
C₂₃H₂₂FNO₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: nitric acid; acetic acid; sulfuric acid / 1 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C

3.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C

3.2: 2 h / 100 °C

4.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C

5.1: hydrazine hydrate / tert-butyl alcohol / 110 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 20 °C

7.1: tetrahydrofuran / 1 h / 0 - 20 °C

8.1: borane-THF / tetrahydrofuran / 0 - 60 °C / Inert atmosphere

9.1: caesium carbonate / butanone / 0.5 h

9.2: 1 h / 20 °C

10.1: aluminum (III) chloride; ethanethiol / dichloromethane / 1 h / 0 - 20 °C

11.1: water; sodium hydroxide / tetrahydrofuran / 0 - 20 °C

With dmap; aluminum (III) chloride; borane-THF; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; nitric acid; caesium carbonate; hydrazine hydrate; acetic acid; triethylamine; trifluoroacetic acid; ethanethiol; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1427406-54-9
C₂₃H₂₂FNO₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1 h / 0 - 20 °C

2.1: nitric acid; acetic acid; sulfuric acid / 1 h / 0 - 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C

4.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C

4.2: 2 h / 100 °C

5.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C

6.1: hydrazine hydrate / tert-butyl alcohol / 110 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 20 °C

8.1: tetrahydrofuran / 1 h / 0 - 20 °C

9.1: borane-THF / tetrahydrofuran / 0 - 60 °C / Inert atmosphere

10.1: caesium carbonate / butanone / 0.5 h

10.2: 1 h / 20 °C

11.1: aluminum (III) chloride; ethanethiol / dichloromethane / 1 h / 0 - 20 °C

12.1: water; sodium hydroxide / tetrahydrofuran / 0 - 20 °C

With dmap; aluminum (III) chloride; borane-THF; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; nitric acid; caesium carbonate; hydrazine hydrate; acetic acid; triethylamine; trifluoroacetic acid; ethanethiol; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; butanone; tert-butyl alcohol;