C₂₃H₃₉NO₃Si

Base Information

Chemical Name:C₂₃H₃₉NO₃Si
CAS No.:1333318-88-9
Molecular Formula:C₂₃H₃₉NO₃Si
Molecular Weight:405.653
Hs Code.:

C<sub>23</sub>H<sub>39</sub>NO<sub>3</sub>Si

Synonyms:C₂₃H₃₉NO₃Si

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Chemical Property of C₂₃H₃₉NO₃Si

Chemical Property:

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Technology Process of C₂₃H₃₉NO₃Si

There total 4 articles about C₂₃H₃₉NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 101166-65-8
2-tert-butyldimethylsilyloxyethyl iodide

: 637767-50-1
pent-4-enoic acid ((1R,2R)-2-hydroxy-1-methyl-2-phenylethyl)-methylamide

: 1333318-88-9
C₂₃H₃₉NO₃Si

Guidance literature:: pent-4-enoic acid ((1R,2R)-2-hydroxy-1-methyl-2-phenylethyl)-methylamide; With lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 1.33333h; Inert atmosphere;

2-tert-butyldimethylsilyloxyethyl iodide; In tetrahydrofuran; hexane; at 0 ℃; for 0.25h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ja2073356

Reference yield:

: 591-80-0
pent-4-enoic acid

: 1333318-88-9
C₂₃H₃₉NO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

3.1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran; hexane / 1.33 h / -78 - 25 °C / Inert atmosphere

3.2: 0.25 h / 0 °C / Inert atmosphere

With pivaloyl chloride; triethylamine; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/ja2073356

Reference yield:

: 178327-16-7
C₄H₇CO₂COC₄H₉

: 1333318-88-9
C₂₃H₃₉NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

2.1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran; hexane / 1.33 h / -78 - 25 °C / Inert atmosphere

2.2: 0.25 h / 0 °C / Inert atmosphere

With lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/ja2073356