1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine

Base Information

• Chemical Name: 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine
• CAS No.: 78815-57-3
• Molecular Formula: C₁₆H₂₁NO₃
• Molecular Weight: 275.348

Synonyms:1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine

Chemical Property of 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine

Chemical Property:

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Technology Process of 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine

There total 2 articles about 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

4-(3-methoxybenzyl)-1-methyl-1,2,3,6-tetrahydropyridine-2-carbonitrile (78815-54-0) → 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-1-methylpyridine (78815-58-4) + 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine (78815-57-3)

Guidance literature:

With hydrogenchloride; In methanol; at 54 ℃; for 60h;

DOI:10.1039/P19810001754

Reference yield: 25.0%

methanol (67-56-1) + 4-(3-methoxybenzyl)-1-methyl-1,2,3,6-tetrahydropyridine-2-carbonitrile (78815-54-0) → 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-1-methylpyridine (78815-58-4) + 1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine (78815-57-3)

Guidance literature:

With hydrogenchloride; at 54 ℃; for 60h;

DOI:10.1039/P19810001754

Reference yield: 73.0%

1,2,3,6-tetrahydro-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpyridine (78815-57-3) → trans-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpiperidine (78815-59-5,78815-60-8) + cis-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpiperidine (78815-59-5,78815-60-8)

Guidance literature:

With hydrogen; platinum on activated charcoal; In acetic acid; for 92h; Ambient temperature;

DOI:10.1039/P19810001754

upstream raw materials:

methanol

4-(3-methoxybenzyl)-1-methyl-1,2,3,6-tetrahydropyridine-2-carbonitrile

Downstream raw materials:

trans-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpiperidine

cis-4-(3-methoxybenzyl)-2-methoxycarbonyl-1-methylpiperidine

2-(1-hydroxy-1-methylethyl)-4-(3-methoxybenzyl)-1-methylpiperidine

4-(3-methoxybenzyl)-1-methylpiperidine

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