2,2’,6,6’-tetrafluoroazobenzene

Base Information

Chemical Name:2,2’,6,6’-tetrafluoroazobenzene
CAS No.:1415919-92-4
Molecular Formula:C₁₂H₆F₄N₂
Molecular Weight:254.187
Hs Code.:

Synonyms:2,2’,6,6’-tetrafluoroazobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2’,6,6’-tetrafluoroazobenzene

Chemical Property:

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Technology Process of 2,2’,6,6’-tetrafluoroazobenzene

There total 6 articles about 2,2’,6,6’-tetrafluoroazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 372-18-9
1,3-Difluorobenzene

: 2,6-difluorobenzene diazonium tetrafluoroborate

: 1415919-92-4
2,2’,6,6’-tetrafluoroazobenzene

Guidance literature:: 1,3-Difluorobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

2,6-difluorobenzene diazonium tetrafluoroborate; In tetrahydrofuran; hexane; at -78 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201607529

Reference yield: 24.0%

: 5509-65-9
2,6-difluoroaniline

: 1415919-92-4
2,2’,6,6’-tetrafluoroazobenzene

Guidance literature:: With ferrous(II) sulfate heptahydrate; potassium permanganate; In dichloromethane; Reflux;
DOI:10.1021/ja310323y

Reference yield:

: 5509-65-9
2,6-difluoroaniline

: 1415919-92-4
2,2’,6,6’-tetrafluoroazobenzene

: cis-1,2-bis(2,6-difluorophenyl)diazene

Guidance literature:: With lead(IV) tetraacetate; In chloroform; at 20 ℃; Overall yield = 38 %; Overall yield = 131 mg; Reflux;
DOI:10.1039/c7cc00961e