3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene

Base Information

Chemical Name:3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene
CAS No.:76999-39-8
Molecular Formula:C₁₅H₂₆OSi
Molecular Weight:250.456
Hs Code.:

3-(2-oxoethyl)-3-<trans-β-(trimethylsilyl)vinyl>-5.5-dimethylcyclohex-1-ene

Synonyms:3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene

Chemical Property:

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Technology Process of 3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene

There total 4 articles about 3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4683-45-8
3-methoxy-5,5-dimethyl-cyclohex-2-enone

: 76999-39-8
3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 50 min; -33 deg C, 50 min, 2.) from -78 deg C to room temp., 4.5 h

2: 96 percent / lithium aluminium hydride / diethyl ether / 4 h / 0 °C

3: 1) Hg(OAc)2 / 1) reflux, several h; 2a) 187 deg C, 5.75 h, b) 200 deg C, 30 min

With lithium aluminium tetrahydride; n-butyllithium; mercury(II) diacetate; In diethyl ether;
DOI:10.1021/jo00324a041

Reference yield:

: 58207-97-9
tributyl[(E)-2-trimethylsilylethenyl]stannane

: 76999-39-8
3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 50 min; -33 deg C, 50 min, 2.) from -78 deg C to room temp., 4.5 h

2: 96 percent / lithium aluminium hydride / diethyl ether / 4 h / 0 °C

3: 1) Hg(OAc)2 / 1) reflux, several h; 2a) 187 deg C, 5.75 h, b) 200 deg C, 30 min

With lithium aluminium tetrahydride; n-butyllithium; mercury(II) diacetate; In diethyl ether;
DOI:10.1021/jo00324a041

Reference yield:

: 76999-36-5
5,5-dimethyl-3-cyclohex-2-en-1-one

: 76999-39-8
3-(2-oxoethyl)-3--5.5-dimethylcyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / lithium aluminium hydride / diethyl ether / 4 h / 0 °C

2: 1) Hg(OAc)2 / 1) reflux, several h; 2a) 187 deg C, 5.75 h, b) 200 deg C, 30 min

With lithium aluminium tetrahydride; mercury(II) diacetate; In diethyl ether;
DOI:10.1021/jo00324a041