2-chlorobenzyl picolinate

Base Information

Chemical Name:2-chlorobenzyl picolinate
CAS No.:438022-98-1
Molecular Formula:C₁₃H₁₀ClNO₂
Molecular Weight:247.681
Hs Code.:

Synonyms:2-chlorobenzyl picolinate

Suppliers and Price of 2-chlorobenzyl picolinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-chlorobenzyl picolinate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2-chlorobenzyl picolinate

There total 1 articles about 2-chlorobenzyl picolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 98-98-6
2-Picolinic acid

: 17849-38-6
2-Chlorobenzyl alcohol

: 438022-98-1
2-chlorobenzyl picolinate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 17h; Inert atmosphere;
DOI:10.1021/jacs.9b13753

Reference yield: 54.0%

: 438022-98-1
2-chlorobenzyl picolinate

: 555-16-8
4-nitrobenzaldehdye

: 118250-41-2
2-chlorobenzyl 4-nitrobenzoate

Guidance literature:: 2-chlorobenzyl picolinate; With palladium diacetate; 1,2-bis-(diphenylphosphino)ethane; In toluene; at 115 ℃; for 0.166667h;

4-nitrobenzaldehdye; With tert.-butylhydroperoxide; In toluene; for 48h; Reflux;
DOI:10.1021/jo3012573

Reference yield:

: 438022-98-1
2-chlorobenzyl picolinate

: 5-amino-2-chlorobenzyl picolinate

: 3-amino-2-chlorobenzyl picolinate

Guidance literature:: With iron(III) chloride; 1,1,1,3',3',3'-hexafluoro-propanol; triethylamine; hydroxylamine-O-sulfonic acid; at 0 - 40 ℃; for 16h; Overall yield = 76 percent; regioselective reaction; Inert atmosphere;
DOI:10.1021/jacs.9b13753