5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide

Base Information

Chemical Name:5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide
CAS No.:338799-88-5
Molecular Formula:C₂₁H₂₂N₂O₂S
Molecular Weight:366.484
Hs Code.:

Synonyms:5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide

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Chemical Property of 5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide

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Technology Process of 5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide

There total 3 articles about 5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-dimethylamino-naphthalene-1-sulfonic acid (4-vinyl-phenyl)-amide

: 74-88-4
methyl iodide

: 338799-88-5
5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 35 - 40 ℃; for 3h;
DOI:10.1021/ja0058435

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 338799-88-5
5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylamino pyridine; pyridine / 1,2-dichloro-ethane / 6 h / 60 - 65 °C

2: 0.908 g / potassium carbonate / dimethylformamide / 3 h / 35 - 40 °C

With pyridine; dmap; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0058435

Reference yield:

: 1520-21-4,25086-42-4
4-vinyl benzylamine

: 338799-88-5
5-dimethylamino-naphthalene-1-sulfonic acid methyl-(4-vinyl-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylamino pyridine; pyridine / 1,2-dichloro-ethane / 6 h / 60 - 65 °C

2: 0.908 g / potassium carbonate / dimethylformamide / 3 h / 35 - 40 °C

With pyridine; dmap; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0058435