2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate

Base Information

Chemical Name:2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate
CAS No.:1372720-45-0
Molecular Formula:C₄₉H₅₀N₂O₇S
Molecular Weight:811.011
Hs Code.:

2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate

Synonyms:2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate

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Chemical Property of 2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate

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Technology Process of 2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate

There total 2 articles about 2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1198587-13-1
4-{[(2-hydroxyethyl)(2-naphthylmethyl)amino]methyl}-N-(tetrahydro-2H-pyran-2-yloxy)benzamide

: 908082-76-8
2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethanol

: 1372720-45-0
2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate

Guidance literature:: 4-{[(2-hydroxyethyl)(2-naphthylmethyl)amino]methyl}-N-(tetrahydro-2H-pyran-2-yloxy)benzamide; With dmap; bis(trichloromethyl) carbonate; In dichloromethane; at 20 ℃; for 0.25h;

2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethanol; In dichloromethane; at 20 ℃; for 7h;
DOI:10.1248/cpb.59.1386

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 1372720-45-0
2-{[(4-methoxyphenyl)(diphenyl)methyl]sulfanyl}ethyl 2-[(2-naphthylmethyl)(4-{[(tetrahydro-2H-pyran-2-yloxy)amino]carbonyl}benzyl)amino]ethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C

2.1: dmap; bis(trichloromethyl) carbonate / dichloromethane / 0.25 h / 20 °C

2.2: 7 h / 20 °C

With dmap; bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.59.1386