(S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

Base Information

Chemical Name:(S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate
CAS No.:1620161-78-5
Molecular Formula:C₁₇H₂₃ClN₂O₅
Molecular Weight:370.833
Hs Code.:

Synonyms:(S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

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Chemical Property of (S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

Chemical Property:

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Technology Process of (S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

There total 1 articles about (S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 27317-69-7
N-tert-butoxycarbonyl-L-alanyl-L-alanine

: 106-48-9,82344-39-6
4-chloro-phenol

: 1620161-78-5
(S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol501669n

Reference yield: 81.0%

: 4306-24-5
Gly-Leu-Tyr

: 1620161-78-5
(S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

: 1620161-81-0
(6S,9S,15S,18S)-18-(4-hydroxybenzyl)-15-isobutyl-2,2,6,9-tetramethyl-4,7,10,13,16-pentaoxo-3-oxa-5,8,11,14,17-pentaazanonadecan-19-oic acid

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 192h; Inert atmosphere;
DOI:10.1021/ol501669n

Reference yield:

: 1620161-78-5
(S)-4-chlorophenyl 2-((S)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

: 1620162-13-1
C₂₉H₃₈N₆O₈S

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 192 h / 20 °C / Inert atmosphere

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ol501669n