Furo2,3-bfuran-3,4-dicarboxylic acid, 2,3,3a,6a-tetrahydro-2-oxo-5,6a-diphenyl-, dimethyl ester, (3.alpha.,3a.alpha.,6a.alpha.)-

Base Information

Chemical Name:Furo2,3-bfuran-3,4-dicarboxylic acid, 2,3,3a,6a-tetrahydro-2-oxo-5,6a-diphenyl-, dimethyl ester, (3.alpha.,3a.alpha.,6a.alpha.)-
CAS No.:90043-46-2
Molecular Formula:C₂₂H₁₈O₇
Molecular Weight:394.381
Hs Code.:

Synonyms:Furo2,3-bfuran-3,4-dicarboxylic acid, 2,3,3a,6a-tetrahydro-2-oxo-5,6a-diphenyl-, dimethyl ester, (3.alpha.,3a.alpha.,6a.alpha.)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Furo2,3-bfuran-3,4-dicarboxylic acid, 2,3,3a,6a-tetrahydro-2-oxo-5,6a-diphenyl-, dimethyl ester, (3.alpha.,3a.alpha.,6a.alpha.)-

Chemical Property:

PSA：88.13000
LogP:2.41610

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Furo2,3-bfuran-3,4-dicarboxylic acid, 2,3,3a,6a-tetrahydro-2-oxo-5,6a-diphenyl-, dimethyl ester, (3.alpha.,3a.alpha.,6a.alpha.)-

There total 3 articles about Furo2,3-bfuran-3,4-dicarboxylic acid, 2,3,3a,6a-tetrahydro-2-oxo-5,6a-diphenyl-, dimethyl ester, (3.alpha.,3a.alpha.,6a.alpha.)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84302-12-5
methyl 2,5-diphenylfuran-3-carboxylate

: 90043-46-2
(3R,3aR,6aS)-2-Oxo-5,6a-diphenyl-2,3,3a,6a-tetrahydro-furo[2,3-b]furan-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: O₂, tetraphenylporphine / tetrahydrofuran / 1 h / -15 °C / Irradiation

2: 1.) NaH / 1.) THF, 2.) 6 h, room temp

With oxygen; 5,15,10,20-tetraphenylporphyrin; sodium hydride; In tetrahydrofuran;
DOI:10.1055/s-1984-30733