3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate

Base Information

Chemical Name:3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate
CAS No.:454646-67-4
Molecular Formula:C₁₆H₂₇N₃O₂
Molecular Weight:293.409
Hs Code.:

Synonyms:3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate

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Chemical Property of 3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate

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Technology Process of 3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate

There total 5 articles about 3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93489-29-3
C₁₀H₁₇NO

: 3-(1H-imidazol-4-yl)-propan-1-ol hydrochloride

: 454646-67-4
3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate

Guidance literature:: C₁₀H₁₇NO; 3-(1H-imidazol-4-yl)-propan-1-ol hydrochloride; In acetonitrile; Reflux;

With ammonia; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.046

Reference yield:

: 90726-03-7
3-cyclohexylpropanamine hydrochloride

: 454646-67-4
3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate

Guidance literature:: Multi-step reaction with 2 steps

1: pyrographite / ethyl acetate / Reflux

2: acetonitrile / Reflux

With pyrographite; In ethyl acetate; acetonitrile;
DOI:10.1016/j.bmc.2011.03.046

Reference yield:

: 1124-63-6
3-cyclohexylpropan-1-ol

: 454646-67-4
3-(1H-imidazol-4-yl)propyl 3-cyclohexylpropylcarbamate hydrogen maleate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: hydrazine hydrate / ethanol / 3 h / Reflux

3: pyrographite / ethyl acetate / Reflux

4: acetonitrile / Reflux

With pyrographite; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; ethyl acetate; acetonitrile; 1: Mitsunobu reaction;
DOI:10.1016/j.bmc.2011.03.046