Benzeneacetic acid, .alpha.-broMo-4-(Methylsulfonyl)-, Methyl ester

Base Information

Chemical Name:Benzeneacetic acid, .alpha.-broMo-4-(Methylsulfonyl)-, Methyl ester
CAS No.:557798-35-3
Molecular Formula:C₁₀H₁₁BrO₄S
Molecular Weight:307.165
Hs Code.:2930909899
Mol file:557798-35-3.mol

Synonyms:bromo-(4-methylsulfonyl-phenyl)-acetic acid methyl ester

Suppliers and Price of Benzeneacetic acid, .alpha.-broMo-4-(Methylsulfonyl)-, Methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Benzeneacetic acid, .alpha.-broMo-4-(Methylsulfonyl)-, Methyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of Benzeneacetic acid, .alpha.-broMo-4-(Methylsulfonyl)-, Methyl ester

There total 3 articles about Benzeneacetic acid, .alpha.-broMo-4-(Methylsulfonyl)-, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.94%

: 300355-18-4
(4-methanesulfonyl-phenyl)-acetic acid methyl ester

: 557798-35-3
bromo-(4-methylsulfonyl-phenyl)-acetic acid methyl ester

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); bromine; In tetrachloromethane; at 80 ℃;

Reference yield:

: 16188-55-9
2-(4-(methylthio)phenyl)acetic acid

: 557798-35-3
bromo-(4-methylsulfonyl-phenyl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 0.25 h

1.2: 24 h / 20 °C

2.1: Oxone / methanol; water / 20 °C / Cooling with ice

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); bromine / tetrachloromethane / 80 °C

With Oxone; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); bromine; sodium hydrogencarbonate; In methanol; tetrachloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 70290-37-8
(4-methylsulfanyl-phenyl)-acetic acid methyl ester

: 557798-35-3
bromo-(4-methylsulfonyl-phenyl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Oxone / methanol; water / 20 °C / Cooling with ice

2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); bromine / tetrachloromethane / 80 °C

With Oxone; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); bromine; In methanol; tetrachloromethane; water;