prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate

Base Information

Chemical Name:prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate
CAS No.:1268809-46-6
Molecular Formula:C₃₀H₃₁NO₅Se
Molecular Weight:564.54
Hs Code.:

Synonyms:prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate

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Chemical Property of prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate

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Technology Process of prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate

There total 6 articles about prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268809-45-5
prop-2-en-1-yl (2R)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methylphenyl)sulfonyl]oxy}methyl)propanoate

: 847354-75-0
(4-methoxy-phenyl)-methaneselenol

: 1268809-46-6
prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate

Guidance literature:: With sodium hydroxide; In water; N,N-dimethyl-formamide; acetone; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1002/hlca.201000409

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1268809-46-6
prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: selenium

2: hypophosphorous acid / tetrahydrofuran / 1 h / Inert atmosphere; Reflux

3: sodium hydroxide / water; N,N-dimethyl-formamide; acetone / 4 h / 0 °C / Inert atmosphere

With selenium; hypophosphorous acid; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.201000409

Reference yield:

: 1268809-43-3
prop-2-en-1-yl (2R)-3-(1,1-dimethylethoxy)-2-[({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)methyl]propanoate

: 1268809-46-6
prop-2-en-1-yl (2S)-3-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-({[(4-methoxyphenyl)methyl]selanyl}methyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl iodide / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: pyridine / 12 h / 0 °C / Inert atmosphere

3: sodium hydroxide / water; N,N-dimethyl-formamide; acetone / 4 h / 0 °C / Inert atmosphere

With pyridine; trimethylsilyl iodide; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.201000409