4-methoxy-N'-methyl-N'-phenylbenzenesulfonohydrazide

Base Information

• Chemical Name: 4-methoxy-N'-methyl-N'-phenylbenzenesulfonohydrazide
• CAS No.: 1391139-05-1
• Molecular Formula: C₁₄H₁₆N₂O₃S
• Molecular Weight: 292.359
• Mol file: 1391139-05-1.mol

Synonyms:4-methoxy-N'-methyl-N'-phenylbenzenesulfonohydrazide

Chemical Property of 4-methoxy-N'-methyl-N'-phenylbenzenesulfonohydrazide

Chemical Property:

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Technology Process of 4-methoxy-N'-methyl-N'-phenylbenzenesulfonohydrazide

There total 1 articles about 4-methoxy-N'-methyl-N'-phenylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-bromo-4-methoxy-benzene (104-92-7) + 1-Methyl-1-phenylhydrazine (618-40-6) → 4-methoxy-N'-methyl-N'-phenylbenzenesulfonohydrazide (1391139-05-1)

Guidance literature:

With potassium pyrosulfite; tetrabutylammomium bromide; palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate; In 1,4-dioxane; at 100 ℃; for 12h;

DOI:10.1039/c2cc34957d

upstream raw materials:

1-bromo-4-methoxy-benzene

1-Methyl-1-phenylhydrazine