methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

Base Information

• Chemical Name: methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate
• CAS No.: 496916-52-0
• Molecular Formula: C₁₉H₂₂FNO₁₀
• Molecular Weight: 443.383

Synonyms:methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

Chemical Property of methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

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Technology Process of methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

There total 3 articles about methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methyl (2-fluoro-4-nitrophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate (496916-51-9) → methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate (496916-52-0)

Guidance literature:

With hydrogen; 10percent Pd/C; In ethanol; at 20 ℃;

DOI:10.1039/b111549a

Reference yield:

2-fluoro-4-nitrophenol (403-19-0) → methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate (496916-52-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / Ag₂O / acetonitrile / 20 °C

2: 85 percent / H₂ / 10percent Pd/C / ethanol / 20 °C

With hydrogen; silver(l) oxide; 10percent Pd/C; In ethanol; acetonitrile;

DOI:10.1039/b111549a

Reference yield:

1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester (21085-72-3) → methyl (2-fluoro-4-aminophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate (496916-52-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / Ag₂O / acetonitrile / 20 °C

2: 85 percent / H₂ / 10percent Pd/C / ethanol / 20 °C

With hydrogen; silver(l) oxide; 10percent Pd/C; In ethanol; acetonitrile;

DOI:10.1039/b111549a

upstream raw materials:

methyl (2-fluoro-4-nitrophenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid)uronate

2-fluoro-4-nitrophenol

1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

Downstream raw materials:

methyl {2-fluoro-4-[bis(2-hydroxyethyl)amino]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

2-fluoro-4-[bis(2-chloroethyl)amino]phenyl β-D-glucopyranosiduronic acid

methyl {2-fluoro-4-[bis(2-chloroethyl)amino]phenyl β-D-glucopyranosid}uronate

methyl {2-fluoro-4-[bis(2-chloroethyl)amino]phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranosid}uronate

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