dimethyl p-acetylbenzyl phosphite

Base Information

Chemical Name:dimethyl p-acetylbenzyl phosphite
CAS No.:181465-68-9
Molecular Formula:C₁₁H₁₅O₄P
Molecular Weight:242.211
Hs Code.:

Synonyms:dimethyl p-acetylbenzyl phosphite

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl p-acetylbenzyl phosphite

Chemical Property:

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Technology Process of dimethyl p-acetylbenzyl phosphite

There total 3 articles about dimethyl p-acetylbenzyl phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 20621-25-4
dimethoxy(diethylamino)phosphine

: 75633-63-5
4-(hydroxymethyl)acetophenone

: 181465-68-9
dimethyl p-acetylbenzyl phosphite

Guidance literature:: With 1H-tetrazole; In acetonitrile; for 18h; Ambient temperature;
DOI:10.1021/ja982440k

Reference yield:

: 51229-51-7
4-acetylbenzyl bromide

: 181465-68-9
dimethyl p-acetylbenzyl phosphite

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / CaCO₃, H₂O / dioxane / 15 h / Heating

2: 86 percent / 1-H-tetrazole / acetonitrile / 18 h / Ambient temperature

With 1H-tetrazole; water; calcium carbonate; In 1,4-dioxane; acetonitrile;
DOI:10.1021/ja982440k

Reference yield:

: 122-00-9
para-methylacetophenone

: 181465-68-9
dimethyl p-acetylbenzyl phosphite

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / NBS, benzoyl peroxide / benzene / 6 h / Irradiation

2: 60 percent / CaCO₃, H₂O / dioxane / 15 h / Heating

3: 86 percent / 1-H-tetrazole / acetonitrile / 18 h / Ambient temperature

With 1H-tetrazole; N-Bromosuccinimide; Perbenzoic acid; water; calcium carbonate; In 1,4-dioxane; acetonitrile; benzene;
DOI:10.1021/ja982440k