(2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)

Base Information

Chemical Name:(2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)
CAS No.:1512624-36-0
Molecular Formula:C₃₂H₄₂N₄O₆
Molecular Weight:578.709
Hs Code.:

Synonyms:(2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)

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Chemical Property of (2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)

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Technology Process of (2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)

There total 1 articles about (2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 92-87-5
p,p'-diaminobiphenyl

: 1512624-36-0
(2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)

Guidance literature:: With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/ardp.201800017

Reference yield: 85.0%

: 1512624-36-0
(2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)

: 1013405-02-1
(2S,2′S)-N,N'-([1,1′-biphenyl]-4,4′-diyl)bis(pyrrolidine-2-carboxamide)

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 4h; Reflux; Inert atmosphere;
DOI:10.1016/j.bmcl.2014.03.015

Reference yield: 36.0%

: 1512624-36-0
(2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate)

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1512624-39-3
dimethyl (2R,2'R)-1,1'-((2S,2'S)-2,2'-(biphenyl-4,4'-diylbis(azandiyl))bis(oxomethylene)bis(pyrrolidine-2,1-diyl))bis(3-methyl-1-oxobutane-2,1-diyl)dicarbamate

Guidance literature:: (2S,2′S)-di-tert-butyl 2,2′-(([1,1′-biphenyl]4,4′diylbis(azanediyl))bis(carbonyl))bis(pyrrolidine-1-carboxylate); With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;

N-methoxycarbonyl-L-valine; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1.31667h;