3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

Base Information

Chemical Name:3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil
CAS No.:1425368-13-3
Molecular Formula:C₂₁H₂₃FN₄O₁₀
Molecular Weight:510.433
Hs Code.:

Synonyms:3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

Suppliers and Price of 3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

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Technology Process of 3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

There total 5 articles about 3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-41-4,25087-26-7,50867-57-7
poly(methacrylic acid)

: C₁₇H₁₉FN₄O₉

: 1425368-13-3
3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

Guidance literature:: With diisopropyl (E)-azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -20 - 20 ℃; for 3.5h;
DOI:10.1016/j.jphotochem.2012.08.012

Reference yield:

: 1150604-93-5
3-hydroxy-4-methoxy-2,6-dinitrobenzyl alcohol

: 1425368-13-3
3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 70 °C

2: diisopropyl (E)-azodicarboxylate; triphenylphosphine / tetrahydrofuran / 15.5 h / -20 - 20 °C

3: hydrogenchloride / methanol / 15 h / 60 °C

4: diisopropyl (E)-azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3.5 h / -20 - 20 °C

With hydrogenchloride; potassium carbonate; diisopropyl (E)-azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.jphotochem.2012.08.012

Reference yield:

: 1425368-09-7
3-(5-(tert-butyldimethylsilyloxy)pentyloxy)-4-methoxy-2,6-dinitrobenzylalcohol

: 1425368-13-3
3-N-(3-(5-methacryloxypentyloxy)-4-methoxy-2,6-dinitrobenzyl)-5-fluorouracil

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropyl (E)-azodicarboxylate; triphenylphosphine / tetrahydrofuran / 15.5 h / -20 - 20 °C

2: hydrogenchloride / methanol / 15 h / 60 °C

3: diisopropyl (E)-azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3.5 h / -20 - 20 °C

With hydrogenchloride; diisopropyl (E)-azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1016/j.jphotochem.2012.08.012