4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate

Base Information

Chemical Name:4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate
CAS No.:127654-92-6
Molecular Formula:C₁₅H₂₅N₂O₃P
Molecular Weight:312.349
Hs Code.:

Synonyms:4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate

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Technology Process of 4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate

There total 2 articles about 4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 127654-91-5
4-Allyl-2-methoxyphenyl N,N,N',N'-tetramethylphosphorodiamidate

: 74-88-4
methyl iodide

: 127654-92-6
4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate

Guidance literature:: With sec.-butyllithium; In tetrahydrofuran; at -105 ℃;

Reference yield:

: 97-53-0
4-allylguaiacol

: 127654-92-6
4-Allyl-2-methoxy-6-methylphenyl N,N,N',N'-tetramethylphosphorodiamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / THF

2: 1.) sec-BuLi / 1.) THF, -105 deg C, 2.) THF

With sec.-butyllithium; sodium hydride;
DOI:10.1248/cpb.39.41