NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3CF₃COO^(1-)=NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5(CF₃COO)3

Base Information

• Chemical Name: NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3CF₃COO^(1-)=NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5(CF₃COO)3
• CAS No.: 81688-57-5
• Molecular Formula: 3C₂F₃O₂*C₁₇H₄₀CoN₈O₄
• Molecular Weight: 818.597

Synonyms:NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3CF₃COO^(1-)=NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5(CF₃COO)3

Chemical Property of NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3CF₃COO^(1-)=NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5(CF₃COO)3

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Technology Process of NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3CF₃COO^(1-)=NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5(CF₃COO)3

There total 1 articles about NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3CF₃COO^(1-)=NH₃CH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5(CF₃COO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

BOC-glycine (4530-20-5) + NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3BF4(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(BF4)3 (81688-54-2) + dicyclohexyl-carbodiimide (538-75-0) + trifluoroacetic acid (76-05-1) → NH3CH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3 (81688-57-5)

Guidance literature:

With 4-methyl-morpholine; In dichloromethane; byproducts: DCU; Boc-Gly was dissolved in CH2Cl2, cooled to 0°C, DCC in CH2Cl2 at0°C was added, stirred for 2 h at 0°C, filtered, filtratewas evapd. to dryness, solid was dissolved in DMF, Co-complex was added, stirred, N-methylmorpholine was adde; reaction was left for 20 min, concd., soln. was stirred with CF3COOH for 1 h at room temp., evapd. to dryness by rotary evaporator, dissolved in EtAc, extd. with aq. HOAc, purified by column chromy., eluted with CF3COOH, evapd. to dryness at room temp.;

DOI:10.1021/ja00378a021

Reference yield: 55.0%

BOC-glycine (4530-20-5) + NH3CH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3 (81688-57-5) + dicyclohexyl-carbodiimide (538-75-0) + trifluoroacetic acid (76-05-1) → NH3CH2CONHCH2CONHCHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-) (81688-60-0)

Guidance literature:

With 4-methyl-morpholine; In dichloromethane; byproducts: DCU; Boc-Gly was dissolved in CH2Cl2, cooled to 0°C, DCC in CH2Cl2 at0°C was added, stirred for 2 h at 0°C, filtered, filtratewas evapd. to dryness, solid was dissolved in DMF, Co-complex was added, stirred, N-methylmorpholine was adde; reaction was left for 30 min, concd., soln. was stirred with CF3COOH for 2 h, evapd. to dryness at room temp., dissolved in EtAc, extd. with aq. HOAc, purified by column chromy., eluted with CF3COOH, evapd. to dryness at room temp.;

DOI:10.1021/ja00378a021

upstream raw materials:

BOC-glycine

NH₃CHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3BF₄^(1-)=NH₃CHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5(BF₄)3

dicyclohexyl-carbodiimide

trifluoroacetic acid

Downstream raw materials:

NH₃CH₂CONHCH₂CONHCHCH₂C₆H₅CONHCHCOOCH₂CH(CH₃)2Co(NH₃)5⁽³⁺⁾*3CF₃COO^(1-)

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