3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol

Base Information

Chemical Name:3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol
CAS No.:1180491-86-4
Molecular Formula:C₂₅H₂₄O₆
Molecular Weight:420.462
Hs Code.:

Synonyms:3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol

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Chemical Property of 3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol

Chemical Property:

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Technology Process of 3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol

There total 8 articles about 3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1180491-74-0
methyl 3-(3,5-dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-carboxylate

: 1180491-86-4
3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃;
DOI:10.1039/b901911a

Reference yield:

: 39151-19-4
1-(3,5-dimethoxyphenyl)ethan-1-one

: 1180491-86-4
3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol

Guidance literature:: Multi-step reaction with 5 steps

1: copper(ll) bromide / chloroform; ethyl acetate / 16 h / Reflux

2: potassium carbonate / acetone / 3 h / 20 °C

3: methanesulfonic acid / dichloromethane / 30 h / 40 °C

4: potassium acetate; palladium diacetate; N,N-dimethyl acetamide / 18 h / 120 °C / Sealed tube

5: magnesium; ammonium chloride / tetrahydrofuran; methanol / 3 h / 0 - 20 °C

With methanesulfonic acid; N,N-dimethyl acetamide; potassium acetate; palladium diacetate; potassium carbonate; ammonium chloride; magnesium; copper(ll) bromide; In tetrahydrofuran; methanol; dichloromethane; chloroform; ethyl acetate; acetone;
DOI:10.1055/s-0035-1561419

Reference yield:

: 50841-50-4
(2-bromo-1-(3,5-dimethoxyphenyl)ethanone)

: 1180491-86-4
3-(3,5-dimethoxyphenyl)-(6-methoxy-2-(4-methoxyphenyl)-benzofuran-4-yl) methanol

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 3 h / 20 °C

2: methanesulfonic acid / dichloromethane / 30 h / 40 °C

3: potassium acetate; palladium diacetate; N,N-dimethyl acetamide / 18 h / 120 °C / Sealed tube

4: magnesium; ammonium chloride / tetrahydrofuran; methanol / 3 h / 0 - 20 °C

With methanesulfonic acid; N,N-dimethyl acetamide; potassium acetate; palladium diacetate; potassium carbonate; ammonium chloride; magnesium; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1055/s-0035-1561419