2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

Base Information

Chemical Name:2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate
CAS No.:107092-32-0
Molecular Formula:C₁₆H₁₃NO₃S₂
Molecular Weight:331.416
Hs Code.:

Synonyms:2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

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Chemical Property of 2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

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Technology Process of 2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

There total 2 articles about 2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 85161-08-6
<4-methoxy(thiobenzoyl)thiomethyl>triphenylphosphonium iodide

: 107092-32-0
2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

: 2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 3h; Yield given. Yields of byproduct given;
DOI:10.1246/bcsj.59.1403

Reference yield:

: 50684-41-8
piperidinium 4-methoxybenzenecarbodithioate

: 107092-32-0
2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / methanol; CH₂Cl₂ / 1 h / Ambient temperature

2: potassium t-butoxide / tetrahydrofuran / 3 h / 0 °C

With potassium tert-butylate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1246/bcsj.59.1403