4-Methoxydithiobenzoic acid ethyl ester

Base Information

Chemical Name:4-Methoxydithiobenzoic acid ethyl ester
CAS No.:942-85-8
Molecular Formula:C10H12OS2
Molecular Weight:212.337
Hs Code.:2930909090
Mol file:942-85-8.mol

Synonyms:ethyl 4-methoxybezenecarbodithioate;ethyl p-dithioanisoate;p-Methoxy-thiobenzoesaeureethylthioester;Benzenecarbodithioic acid,4-methoxy-,ethyl ester;Ethyl-p-methoxydithiobenzoat;p-Anisic acid,dithio-,ethyl ester;p-Methoxy-dithiobenzoesaeureethylester;4-Methoxy-dithiobenzoesaeure-aethylester;4-Methoxy-dithiobenzoesaeure-ethylester;

Suppliers and Price of 4-Methoxydithiobenzoic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-Methoxydithiobenzoic acid ethyl ester

Chemical Property:

PSA：66.62000
LogP:3.12380

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Methoxydithiobenzoic acid ethyl ester

There total 9 articles about 4-Methoxydithiobenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 54669-43-1
potassium ethanethiolate

: 107092-32-0
2-(4-nitrophenyl)vinyl 4-methoxybezenecarbonditioate

: 942-85-8
ethyl 4-methoxybezenecarbodithioate

: 101482-10-4
<2-(4-Nitrophenyl)vinyl> phenacyl sulfide

Guidance literature:: In tetrahydrofuran; ethanethiol; -70 deg C, 1 h then -10 deg C, 1 h;
DOI:10.1246/bcsj.59.1403

Reference yield:

: 50684-41-8
piperidinium 4-methoxybenzenecarbodithioate

: 942-85-8
ethyl 4-methoxybezenecarbodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / methanol; CH₂Cl₂ / 1 h / Ambient temperature

2: potassium t-butoxide / tetrahydrofuran / 3 h / 0 °C

3: 81 percent / tetrahydrofuran; C₂H₅SH / -70 deg C, 1 h then -10 deg C, 1 h

With potassium tert-butylate; In tetrahydrofuran; methanol; dichloromethane; ethanethiol;
DOI:10.1246/bcsj.59.1403

Reference yield:

: 85161-08-6
<4-methoxy(thiobenzoyl)thiomethyl>triphenylphosphonium iodide

: 942-85-8
ethyl 4-methoxybezenecarbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium t-butoxide / tetrahydrofuran / 3 h / 0 °C

2: 81 percent / tetrahydrofuran; C₂H₅SH / -70 deg C, 1 h then -10 deg C, 1 h

With potassium tert-butylate; In tetrahydrofuran; ethanethiol;
DOI:10.1246/bcsj.59.1403