C₂₈H₄₇NO₄

Base Information

Chemical Name:C₂₈H₄₇NO₄
CAS No.:1292308-82-7
Molecular Formula:C₂₈H₄₇NO₄
Molecular Weight:461.685
Hs Code.:

C<sub>28</sub>H<sub>47</sub>NO<sub>4</sub>

Synonyms:C₂₈H₄₇NO₄

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Chemical Property of C₂₈H₄₇NO₄

Chemical Property:

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Technology Process of C₂₈H₄₇NO₄

There total 12 articles about C₂₈H₄₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₄₇NO₇S

: 75-16-1
methylmagnesium bromide

: 1292308-82-7
C₂₈H₄₇NO₄

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 12.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.01.027

Reference yield:

: 1001208-19-0
(2S,4R)-5-(tert-butyldiphenylsilyloxy)-N-((1R,2R)-1-hydroxy-1-phenylpropan-2-yl)-N,2,4-trimethylpentanamide

: 1292308-82-7
C₂₈H₄₇NO₄

Guidance literature:: Multi-step reaction with 7 steps

1: LAB / tetrahydrofuran / Inert atmosphere

2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / Inert atmosphere

3: n-butyllithium / tetrahydrofuran / Inert atmosphere

4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 14 h / 20 - 40 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

6: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

7: copper(l) iodide / tetrahydrofuran; diethyl ether / 12.5 h / -78 - 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(l) iodide; n-butyllithium; tetrapropylammonium perruthennate; tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2011.01.027

Reference yield:

: 1292309-75-1
C₁₉H₂₉NO₃

: 1292308-82-7
C₂₈H₄₇NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 0 - 20 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 14 h / 20 - 40 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

5: copper(l) iodide / tetrahydrofuran; diethyl ether / 12.5 h / -78 - 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2011.01.027