4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate

Base Information

Chemical Name:4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate
CAS No.:941584-96-9
Molecular Formula:C₂₀H₁₇N₃O₁₀S₂
Molecular Weight:523.501
Hs Code.:

Synonyms:4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate

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Chemical Property of 4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate

Chemical Property:

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Technology Process of 4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate

There total 1 articles about 4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 104-14-3,1915-83-9
octopamine

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 941584-96-9
4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate

Guidance literature:: octopamine; With sodium hydroxide; In 1,4-dioxane; water; at 20 ℃; for 0.0833333h;

2-Nitrobenzenesulfonyl chloride; In 1,4-dioxane; water; at 20 ℃; for 17h;

Reference yield:

: 941584-96-9
4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate

: 101166-65-8
2-tert-butyldimethylsilyloxyethyl iodide

: C₂₈H₃₅N₃O₁₁S₂Si

Guidance literature:: 4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

2-tert-butyldimethylsilyloxyethyl iodide; In N,N-dimethyl-formamide; at 20 - 100 ℃; for 21h;

Reference yield:

: 941584-96-9
4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate

: 101166-65-8
2-tert-butyldimethylsilyloxyethyl iodide

: C₂₈H₃₅N₃O₁₁S₂Si

Guidance literature:: 4-(1-Hydroxy-2-(2-nitrophenylsulfonamido)ethyl)phenyl 2-nitrobenzenesulfonate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

2-tert-butyldimethylsilyloxyethyl iodide; In N,N-dimethyl-formamide; at 100 ℃; for 21h;

With sodium hydrogencarbonate; In N,N-dimethyl-formamide;