diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate

Base Information

Chemical Name:diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate
CAS No.:852948-67-5
Molecular Formula:C₂₆H₃₆Cl₂NO₇P
Molecular Weight:576.454
Hs Code.:

Synonyms:diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate

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Chemical Property of diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate

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Technology Process of diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate

There total 2 articles about diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 852948-66-4
3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

: 106938-62-9
(diethoxyphosphinyl)methyl trifluoromethanesulfonate

: 852948-67-5
diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate

Guidance literature:: 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

(diethoxyphosphinyl)methyl trifluoromethanesulfonate; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield:

: 155891-93-3
(3,5-Dichloro-4-hydroxy-phenyl)-carbamic acid tert-butyl ester

: 852948-67-5
diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper; triethylamine / dichloromethane / 14 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 2 h / 20 °C

With copper; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;