3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

Base Information

Chemical Name:3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester
CAS No.:852948-66-4
Molecular Formula:C₂₁H₂₅Cl₂NO₄
Molecular Weight:426.34
Hs Code.:

Synonyms:3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

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Chemical Property of 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

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Technology Process of 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

There total 1 articles about 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 155891-93-3
(3,5-Dichloro-4-hydroxy-phenyl)-carbamic acid tert-butyl ester

: bis(3-isopropyl-4-methoxyphenyl)iodonium tetrafluoroborate

: 852948-66-4
3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

Guidance literature:: With copper; triethylamine; In dichloromethane; at 0 - 20 ℃; for 14h;

Reference yield: 63.0%

: 852948-66-4
3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

: 106938-62-9
(diethoxyphosphinyl)methyl trifluoromethanesulfonate

: 852948-67-5
diethyl N-tert-butoxycarbonyl-[3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylamino]methylphosphonate

Guidance literature:: 3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

(diethoxyphosphinyl)methyl trifluoromethanesulfonate; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield:

: 852948-66-4
3,5-dichloro-4-(3'-iso-propyl-4'-methoxyphenoxy)phenylcarbamic acid tert-butyl ester

: C₁₇H₂₀Cl₂NO₅P

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 2 h / 20 °C

2.1: trimethylsilyl bromide / dichloromethane / 16 h / 0 - 20 °C

With trimethylsilyl bromide; sodium hydride; In tetrahydrofuran; dichloromethane;