1-Ethoxyoctane

Base Information

• Chemical Name: 1-Ethoxyoctane
• CAS No.: 929-61-3
• Molecular Formula: C10H22 O
• Molecular Weight: 158.284
• Hs Code.: 2909199090
• DSSTox Substance ID: DTXSID10275929
• Nikkaji Number: J137.021I
• Wikidata: Q3591982
• Mol file: 929-61-3.mol

Synonyms:Ether,ethyl octyl (7CI,8CI); Ethyl n-octyl ether; Ethyl octyl ether; Octyl ethylether

Chemical Property of 1-Ethoxyoctane

Chemical Property:

• Vapor Pressure: 0.899mmHg at 25°C
• Melting Point: 12.5°C
• Refractive Index: 1.415
• Boiling Point: 186.7°C at 760 mmHg
• Flash Point: 56.9°C
• PSA: 9.23000
• Density: 0.791g/cm³
• LogP: 3.38340
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 8
• Exact Mass: 158.167065321
• Heavy Atom Count: 11
• Complexity: 61.9

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCOCC

Technology Process of 1-Ethoxyoctane

There total 19 articles about 1-Ethoxyoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

Dimethylphenylsilane (766-77-8) + α-Ethoxyethyl octyl ether (54889-49-5) → ethyl octyl ether (929-61-3) + dimethyl(oct-1-yloxy)(phenyl)silane

Guidance literature:

With aluminum (III) chloride; In dichloromethane; at 0 ℃; chemoselective reaction;

DOI:10.1039/c4ra00655k

Reference yield: 28.0%

→ 3-(4-cyclopentyl-2-thiazolyl)methoxybenzoic acid + ethyl octyl ether (929-61-3)

Guidance literature:

Reference yield: 25.0%

4-tetrahydrofuran-2-yl-butan-2-ol (3208-43-3,4527-76-8) → octanol (111-87-5) + ethyl octyl ether (929-61-3) + di-n-octyl ether (629-82-3)

Guidance literature:

With hydrogen; 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide; at 150 ℃; for 4h; under 90009 Torr; Autoclave;

DOI:10.1039/c4sc02033b

upstream raw materials:

n-octyl methanesulfonate

ethanol

carbon monoxide

1-Iodooctane

Downstream raw materials:

Octanoic acid

octanoic acid ethyl ester

nonanoic acid methyl ester

octyl octylate

Refernces

• 1、 Guilera, Jordi,Hanková, Libuse,Jerabek, Karel,Ramírez, Eliana,Tejero, Javier. "Influence of the functionalization degree of acidic ion-exchange resins on ethyl octyl ether formation". . p. 14 - 22. Retrieved 2014/04/03.
• 2、 Tunbridge, Gemma A.,Baruchello, Riccardo,Caggiano, Lorenzo. "Mild and efficient capture and functionalisation of CO2 using silver(i) oxide and application to 13C-labelled dialkyl carbonates". . p. 4613 - 4621. Retrieved 2013/05/08.